()-1,2,3,4,5,6,7,8-octahydro-1-[(4-methoxyphenyl)methyl]-2-methylisoquinoline
- Name ()-1,2,3,4,5,6,7,8-octahydro-1-[(4-methoxyphenyl)methyl]-2-methylisoquinoline
- CAS 38969-65-2
- Purity 99%
Product Details
Quality manufacturer supply ()-1,2,3,4,5,6,7,8-octahydro-1-[(4-methoxyphenyl)methyl]-2-methylisoquinoline 38969-65-2 in stock with high standard
- Molecular Formula: C18H25 N O
- Molecular Weight: 271.403
- Vapor Pressure: 1.55E-06mmHg at 25°C
- Boiling Point: 397.8°Cat760mmHg
- Flash Point: 117°C
- Density: 1.06g/cm3
38969-65-2 Relevant articles
Preparation method of 1-(4-methoxy-benzyl)-2-methyl-octahydro isoquinoline
-
Paragraph 0028-0033, (2020/06/20)
The invention discloses a preparation me...
Preparation of useful intermediates of dextrorphan - Note I
Passarotti,Valenti,Grianti
, p. 472 - 474 (2007/10/02)
Dextrorphan is the main metabolite of De...
Selective catalytic hydrogenations and hydrogenolyses, VI: An improved synthesis of 1-benzyl-2-methyloctahydroisoquinolines
Reimann,Hoglmuller
, p. 685 - 690 (2007/10/02)
-
Process of N-demethylating (-)-1-(p-methoxybenzyl)-2-methyl-1,2,3,4,5,6,7,8-octahydroisoquinoline
-
, (2008/06/13)
N-Alkyl allylic tertiary amines are deal...
38969-65-2 Process route
-
-
50-00-0,30525-89-4,61233-19-0
formaldehyd
-
-
51072-36-7,57849-23-7
(+)-1-(p-methoxybenzyl)-1,2,3,4,5,6,7,8-octahydroisoquinoline
-
-
38969-65-2,31414-58-1
1-(p-methoxybenzyl)-2-methyl-1,2,3,4,5,6,7,8-octahydroisoquinoline
| Conditions | Yield |
|---|---|
|
formaldehyd; (+)-1-(p-methoxybenzyl)-1,2,3,4,5,6,7,8-octahydroisoquinoline;
In
ethanol;
at 25 ℃;
for 4h;
With
5%-palladium/activated carbon; hydrogen;
In
ethanol;
at 20 ℃;
for 8h;
under 13501.4 Torr;
Reagent/catalyst;
Temperature;
Pressure;
|
95%
|
|
With
methanol; water;
Nachfolgenden Hydrieren an Raney-Nickel;
|
-
-
98237-33-3
1-(4-Methoxybenzyl)-2-methyl-5,6,7,8-tetrahydroisochinoliniumiodide
-
-
38969-65-2,31414-58-1
1-(p-methoxybenzyl)-2-methyl-1,2,3,4,5,6,7,8-octahydroisoquinoline
| Conditions | Yield |
|---|---|
|
With
sodium hydroxide; iodine; platinum;
Hydrogenation;
|
|
|
With
sodium hydroxide; sodium tetrahydroborate;
In
ethanol;
for 15h;
Yield given;
Ambient temperature;
|
38969-65-2 Upstream products
-
118646-97-2
1-(4-methoxy-benzyl)-2-methyl-1,2,3,4,6,7,8,8a-octahydro-isoquinoline
-
118646-96-1
(2-cyclohex-1-enyl-ethyl)-(4-methoxy-styryl)-methyl-amine
-
98237-33-3
1-(4-Methoxybenzyl)-2-methyl-5,6,7,8-tetrahydroisochinoliniumiodide
-
50-00-0
formaldehyd
38969-65-2 Downstream products
-
23667-36-9
6-methyl-2,3,3a,4,5,6,6a,7,11b,11c-decahydro-1H -dibenzo[de ,g ]quinolin-10-ol
-
77-07-6
racemorphan
-
23667-36-9
(+/-)-6-methyl-(3ar ,6at ,11bt ,11ct )-2,3,3a,4,5,6,6a,7,11b,11c-decahydro-1H -dibenzo[de,g ]quinolin-10-ol
-
125-70-2
rac -3-methoxy-17-methyl-morphinane